CD Skripsi
Sintesis Dan Karakterisasi Nanopartikel Zno Menggunakan Ekstrak Daun Ketapang Untuk Mendegradasi Metilen Biru
Synthesis and characterization of ZnO nanoparticles have been successfully
carried out using ketapang leaf extract to degrade methylene blue. ZnO
nanoparticles were formed through the synthesis of a 0.05 M solution of
ZnO(NO3)2 with ketapang leaf extract. The synthesis was carried out using
variations in the volume of the ketapang leaf extract and zinc nitrate solution,
namely A (1:3), B (1:5) and C (1:7) and then 1 M NaOH was added until each
variation showed a pH of 12. The results were characterized using UV-Vis
Spectrophotometer resulting in absorbance values of 0.619; 1.196 and 1.095. Xray
diffraction (XRD) characterization of sample B showed that the particle size is
in the range of 10.59-23.73 nm with Miller indices of (100); (002); (101); (012) ;
(110); (013) and (112). SEM characterization showed the presence of nanoflower
morphology with size distribution in the range of 400-494 nm. The
degradation activity of methylene blue for absorption test using UV-Vis
Spectrophotometer at a concentration of 25 ppm with an optimum time of 6 hours
resulted in the degradation efficiency of 29 %, 32,2 % and 36,7 %.
Key Words : ZnO nanoparticles, Ketapang leaf, Methylene Blue, UV-Vis, XRD,
SEM
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