CD Tesis

kinetika pertumbuhan kristal hidroksiapatit dari precipitated calcium carbonate (pcc) kulit telur ayam secara hidrotermal

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In Indonesia, the incidence of bone fractures in 2018 reached
approximately nine million cases, with various types and causes. Hydroxyapatite
(Ca₁₀(PO₄)₆(OH)₂ or HAp) is one of the bioceramics commonly used in
biomedical applications due to its biocompatible and osteoconductive properties,
allowing it to integrate well with bone.
This study aims to determine the time required for hydroxyapatite (HAp)
production by observing the crystal growth of HAp from chicken eggshells. The
objective of this research is to examine the effect of reaction temperature (120 and
140°C) and hydrothermal reaction time (1, 3, 4, 5, 7, and 9 hours) on the crystal
growth of apatite compounds derived from Precipitated Calcium Carbonate
(PCC) of chicken eggshells. Technically, PCC has advantages such as small
particle size (microscale) and high homogeneity.
HAp is synthesized from PCC and diammonium hydrogen phosphate
((NH₄)₂HPO₄) as a phosphate source in a hydrothermal reactor. The produced
HAp is characterized using X-ray diffraction (XRD). The obtained HAp crystals
have a hexagonal shape with high precision in crystalline details, resembling
Holly Springs hydroxyapatite. The optimal condition for producing the largest
HAp crystal diameter was achieved at a temperature of 140°C, measuring 33.29
nm, with a reaction time of 9 hours. Thus, the higher the reaction temperature and
the longer the synthesis time, the larger the resulting HAp crystal diameter.
Keywords: Bone, Eggshells, Precipitated Calcium Carbonate, Hidroxyapatite

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Ketersediaan

Informasi Detail

Judul Seri

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No. Panggil

2010241973

Penerbit

Pekanbaru : UNRI – PASCA – Magister Teknik Kimia., 2025

Deskripsi Fisik

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Bahasa

Indonesia

ISBN/ISSN

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Klasifikasi

2010241973

Tipe Isi

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Tipe Media

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Tipe Pembawa

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Edisi

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Subjek

Magister Teknik Kimia

Info Detail Spesifik

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Pernyataan Tanggungjawab

Rahmat

Versi lain/terkait

Lampiran Berkas

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